{"id":37453,"date":"2020-04-13T11:06:31","date_gmt":"2020-04-13T03:06:31","guid":{"rendered":"http:\/\/www.chemhui.com\/?p=37453"},"modified":"2020-12-06T11:33:51","modified_gmt":"2020-12-06T03:33:51","slug":"37453","status":"publish","type":"post","link":"http:\/\/www.chemhui.com\/37453\/","title":{"rendered":"\u4e0a\u6d77\u5730\u533a\u2014\u6838\u78c1\u5171\u632f\u6ce2\u8c31\u4eea\u63d0\u4f9b\u6d4b\u8bd5\u670d\u52a1 \u6c22\u8c31\u5355\u6b21\u6d4b\u6837\u6570\u8d85\u8fc720\u4e2a\uff0c\u53ef20\u5143\/\u4e2a"},"content":{"rendered":"

\n\t\u4e0a\u6d77\u5730\u533a\u5b89\u6377\u4f26400\u5146\u6838\u78c1\u5171\u632f\u6ce2\u8c31\u4eea\u63d0\u4f9b\u6d4b\u8bd5\u670d\u52a1<\/b>\n<\/p>\n

\n\t1. <\/b>\u9879\u76ee\uff1a\u6c22\u8c31\u3001\u78b3\u8c31\u3001\u78b3\u8c31deft 135o<\/sup>\u3001H-H COSY\u3001H-H TOCSY\u3001H-H NOESY\u3001H-C
\nHSQC\u3001H-C HMQC<\/b>\n<\/p>\n

\n\t <\/b>\u53ef\u6d4b\uff1a\u6c22\uff0c\u78b3\uff0c\u6c1f\uff0c\u78f7\uff0c\u6db2\u4f53\u6837\u54c1<\/b>\n<\/p>\n

\n\t2. <\/b>\u6d4b\u8bd5\u6536\u8d39\uff1a\u6c22\u8c31 25\u5143\uff0c\u6c1f\u8c3120\u5143\uff0c\u78f7\u8c31 20\u5143\uff0c\u78b3\u8c31\u7c7b 50\u5143\uff08\u6d53\u5ea6\u8981\u8fbe\u5230\u6807\u51c6\u6d53\u5ea6\uff1a\u5206\u5b50\u91cf\u4e0d\u5927\u4e8e1000\u65f660mg\/mL\uff09 \u82e5\u6240\u6d4b\u78b3\u8c31\u7c7b\u6838\u78c1\u6837\u54c1\u6d53\u5ea6\u8fc7\u4f4e\uff0c\u6309\u626b\u63cf\u65f6\u95f4\u6536\u8d39\u8d85\u8fc730\u5206\u949f\u6bcf\u6839100\uff0c\u8d85\u8fc71\u5c0f\u65f6\u540e\u7eed\u65f6\u95f4\u6309\u6bcf\u5c0f\u65f6100\u6536\u8d39\uff0c\u8d85\u8fc73\u5c0f\u65f6\u53ef\u626b\u8fc7\u591c\u6838\u78c1\uff08\u8fc7\u591c\u6838\u78c1300\u5143\uff09\u3002{\u6c18\u4ee3\u6eb6\u5242\u8d39\u6c2f\u4eff\uff0c\u6c34\uff0c\u4e8c\u6c2f\u7532\u70f7\uff0c\u52a0\u65363\u5143\uff0c\u5176\u4ed6\u7684\u52a0\u65365\u5143\uff0c\u5982\u82ef\uff0c\u4e59\u8148\uff0c\u7532\u82ef\uff0c\u7532\u9187\uff0c\u4e19\u916e\uff0cDMSO\u3002\u6211\u4eec\u90fd\u7528\u53ea\u88c5\u7684\u6c18\u4ee3\u8bd5\u5242\uff0c\u4fdd\u8bc1\u8d28\u91cf}<\/b>\n<\/p>\n

\n\t\u4e8c\u7ef4\u8c31\u56fe\u6309\u65f6\u95f4\u6536\u8d391\u5c0f\u65f6200\uff0c\u4e8c\u7ef4\u8c31\u56fe\u7528\u5e03\u9c81\u514b600\u5146\u6d4b\u8bd5 \u3002<\/b>\n<\/p>\n

\n\t\u8d39\u7528\u7ed3\u7b97\uff1a\u6ee11000\u5143\u7ed3\u7b97\u4e00\u6b21\uff08\u5f00\u53d1\u7968\u7684\u8bdd\uff09\u53d1\u7968\u4f4e\u4e8e1000\u53d1\u7968\u8fd0\u8d39\u81ea\u7406<\/b>\n<\/p>\n

\n\t\u6c22\u8c31\u5355\u6b21\u6d4b\u6837\u6570\u8d85\u8fc720\u4e2a\uff0c\u53ef20\u5143\/\u4e2a<\/b>\n<\/p>\n

\n\t3. <\/b>\u6536\u6837\u5730\u5740\uff1a\u79c1\u804a<\/b>\n<\/p>\n

\n\t4. <\/b>\u6d4b\u8bd5\u8d39\u7528\u652f\u4ed8\u65b9\u5f0f\uff1a\u53ef\u8f6c\u8d26\uff0c\u53ef\u5f00\u53d1\u7968\uff08\u52a0\u65368%\u7a0e\u8d39\uff09<\/b>\n<\/p>\n

\n\t5. <\/b>\u8054\u7cfb\u65b9\u5f0f\uff1aQQ\u6216\u5fae\u4fe1\uff1a296921390 <\/b>\n<\/p>\n

6. \u6c22\u8c31\uff0c\u78f7\u8c31\uff0c\u6c1f\u8c31
\n\u5f53\u5929\u6536\u5230\u6837\u53ef\u5f53\u5929\u6d4b\u5b8c\uff0c\u5176\u4ed6\u8c31\u56fe\u770b\u60c5\u51b5\u800c\u5b9a<\/b><\/p>\n","protected":false},"excerpt":{"rendered":"

\u4e0a\u6d77\u5730\u533a\u5b89\u6377\u4f26400\u5146\u6838\u78c1\u5171\u632f\u6ce2\u8c31\u4eea\u63d0\u4f9b\u6d4b\u8bd5\u670d\u52a1 1. \u9879\u76ee\uff1a\u6c22\u8c31\u3001\u78b3\u8c31\u3001\u78b3\u8c31deft 135o\u3001H-H CO […]<\/p>\n","protected":false},"author":5162,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[6],"tags":[],"class_list":["post-37453","post","type-post","status-publish","format-standard","hentry","category-ceshiziyuan"],"_links":{"self":[{"href":"http:\/\/www.chemhui.com\/wp-json\/wp\/v2\/posts\/37453","targetHints":{"allow":["GET"]}}],"collection":[{"href":"http:\/\/www.chemhui.com\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"http:\/\/www.chemhui.com\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"http:\/\/www.chemhui.com\/wp-json\/wp\/v2\/users\/5162"}],"replies":[{"embeddable":true,"href":"http:\/\/www.chemhui.com\/wp-json\/wp\/v2\/comments?post=37453"}],"version-history":[{"count":12,"href":"http:\/\/www.chemhui.com\/wp-json\/wp\/v2\/posts\/37453\/revisions"}],"predecessor-version":[{"id":41064,"href":"http:\/\/www.chemhui.com\/wp-json\/wp\/v2\/posts\/37453\/revisions\/41064"}],"wp:attachment":[{"href":"http:\/\/www.chemhui.com\/wp-json\/wp\/v2\/media?parent=37453"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"http:\/\/www.chemhui.com\/wp-json\/wp\/v2\/categories?post=37453"},{"taxonomy":"post_tag","embeddable":true,"href":"http:\/\/www.chemhui.com\/wp-json\/wp\/v2\/tags?post=37453"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}